農(nóng)藥獸藥多組分殘留質(zhì)譜分析技術(shù)：第1卷.農(nóng)藥

Main Researchers/Editors xiii
Preface xv
Brief Introduction xvii

1. Introduction 1
1.1 Insecticides 1
1.1.1 Organophosphate Insecticides 1
1.1.2 Carbamate Insecticides 2
1.1.3 Organochlorine Insecticides 2
1.1.4 Pyrethroid Insecticides 2
1.1.5 Neonicotinoid Insecticides 2
1.2 Herbicides 3
1.2.1 Phenolic Herbicides 3
1.2.2 Phenoxy Acid Herbicides 3
1.2.3 Benzoic Acid Herbicides 4
1.2.4 Diphenyl Ether Herbicides 4
1.2.5 Dinitroaniline Herbicides 4
1.2.6 Amide Herbicides 4
1.2.7 Carbamate Herbicides 5
1.2.8 Thiocarbamate Herbicides 5
1.2.9 Urea Herbicides 5
1.2.10 Sulfonylurea Herbicides 5
1.2.11 S-Triazine Herbicides 5
1.2.12 Quaternary Ammoniums Herbicides 6
1.2.13 Organophosphate Herbicides 6
1.2.14 Other Herbicides 6
1.3 Bactericides 6
1.3.1 Triazole Bactericides 7
1.3.2 Amide Bactericides 7
1.3.3 Pyridinamine Bactericides 7
1.3.4 Strobin Bactericides 7
1.3.5 Oxazo Bactericides 8
1.3.6 Pyrrole Bactericides 8
1.3.7 Amino Acid Bactericides 8
1.3.8 Derivants of Cinnamic Acid 8
1.3.9 Others 8
1.4 Pesticides Banned in the World 8
1.4.1 Pesticides Banned in China 8
1.4.2 Pesticides Banned in Japan 9
1.4.3 Pesticides Banned in European Union 9

2. Analytical Methods for 793 Pesticides and Related
Chemical Residues in Products of Plant Origin 11
2.1 Determination of 512 Pesticides and Related Chemical Residues
in Fruit Juice and Wine: LC-MS-MS Method (GB/T 23206-2008) 11
2.1.1 Scope 11
2.1.2 Principle 11
2.1.3 Reagents and Materials 11
2.1.4 Apparatus 21
2.1.5 Sample Pretreatment 21
2.1.6 Determination 22
2.1.7 Precision 24
Researchers 24
2.2 Determination of 500 Pesticides and Related Chemical Residues
in Fruits and Vegetables: GC-MS Method (GB/T 19648-2006) 25
2.2.1 Scope 25
2.2.2 Principle 25
2.2.3 Reagents and Materials 25
2.2.4 Apparatus 35
2.2.5 Sample Pretreatment 35
2.2.6 GC-MS Determination 36
2.2.7 Precision 37
Researchers 37
2.3 Determination of 450 Pesticides and Related Chemical Residues
in Fruits and Vegetables: LC-MS-MS Method(GB/T 20769-2008) 37
2.3.1 Scope 37
2.3.2 Principle 45
2.3.3 Reagents and Materials 45
2.3.4 Apparatus 46
2.3.5 Sample Pretreatment 46
2.3.6 Determination 47
2.3.7 Precision 49
Researchers 50
2.4 Determination of 475 Pesticides and Related Chemical Residues
in Grains: GC-MS Method (GB/T 19649-2006) 50
2.4.1 Scope 50
2.4.2 Principle 50
2.4.3 Reagents and Materials 50
2.4.4 Apparatus 59
2.4.5 Sample Pretreatment 59
2.4.6 GC-MS Method Determination 60
2.4.7 Precision 61
Researchers 61
2.5 Determination of 486 Pesticides and Related Chemical Residues
in Grains: LC-MS-MS Method (GB/T 20770-2008) 61
2.5.1 Scope 61
2.5.2 Principle 69
2.5.3 Reagents and Materials 69
2.5.4 Apparatus 71
2.5.5 Sample Pretreatment 71
2.5.6 Determination 72
2.5.7 Precision 73
Researchers 73
2.6 Determination of 519 Pesticides and Related Chemical
Residues in Tea Leaves: GC-MS Method (GB/T 23204-2008) 74
2.6.1 Scope 74
2.6.2 Determination of 490 Pesticides and Related Chemical Residues in Tea: GC-MS Method 74
2.6.3 Determination of 29 Acidic Herbicides in Tea:GC-MS Method 85
Researchers 91
2.7 Determination of 448 Pesticides and Related Chemical
Residues in Tea Leaves: LC-MS-MS Method (GB/T23205-2008) 92
2.7.1 Scope 92
2.7.2 Principle 92
2.7.3 Reagents and Materials 92
2.7.4 Apparatus 101
2.7.5 Sample Pretreatment 101
2.7.6 Determination 102
2.7.7 Precision 103
Researchers 103
2.8 Determination of 488 Pesticides and Related Chemical
Residues in Mulberry Twig, Honeysuckle, Barbary Wolfberry
Fruit, and Lotus Leaf: GC-MS Method (GB/T 23200-2008) 103
2.8.1 Scope 103
2.8.2 Principle 104
2.8.3 Reagents and Materials 104
2.8.4 Apparatus 113
2.8.5 Sample Pretreatment 113
2.8.6 Determination 114
2.8.7 Precision 115
Researchers 115