基礎(chǔ)化學(xué)實驗（中英對照版 第3版）

第一部分 基礎(chǔ)化學(xué)實驗基本知識 第一章 實驗室規(guī)則及安全知識 1.基礎(chǔ)化學(xué)實驗?zāi)康? 2.化學(xué)實驗室一般規(guī)則 3.化學(xué)實驗室的安全知識 4.化學(xué)實驗操作過程中可能發(fā)生的事故與處理 5.化學(xué)實驗室的防火與滅火常識 第二章 基礎(chǔ)化學(xué)實驗常用儀器 1.實驗室常用玻璃儀器 1.1 玻璃儀器的洗滌 1.2 玻璃儀器的干燥 2.容量分析儀器 2.1 滴定管 2.2 容量瓶 2.3 移液管和吸量管 3.常用定量分析儀器 3.1 分析天平 3.2 pH計 3.3 721型分光光度計 3.4 FM-9X型冰點滲透壓計 3.5 離心機 第三章 實驗結(jié)果的表示 1.實驗誤差與有效數(shù)字 1.1 實驗誤差 1.2 準(zhǔn)確度和精密度 1.3 有效數(shù)字 2.實驗數(shù)據(jù)的處理 2.1 列表法 2.2 作圖法 2.3 計算機處理 3.實驗報告 第二部分 基礎(chǔ)化學(xué)實驗課題 實驗課題一 基本操作訓(xùn)練實驗 實驗一 常用容量分析儀器操作練習(xí) 實驗二 分析天平稱量練習(xí) 實驗三 緩沖溶液的配制和性質(zhì)、溶液pH測量 實驗四 膠體溶液的制備與性質(zhì) 實驗課題二 滴定分析實驗 實驗五 酸堿滴定分析法 1.標(biāo)準(zhǔn)鹽酸溶液濃度的標(biāo)定 2.標(biāo)準(zhǔn)氫氧化鈉溶液濃度的標(biāo)定 3.草酸純度的測定 4.硼砂含量的測定 5.返滴定法測定阿司匹林的含量 實驗六 氧化還原滴定法 1.高錳酸鉀法 2.碘量法 實驗七 配位滴定分析 1.水的硬度的測定 2.明礬含量的測定 3.葡萄糖酸鈣含量的測定 實驗課題三 分光光度法實驗 實驗八 分光光度法測定水樣中鐵含量 1.鄰二氮菲法 2.硫氰酸鹽法 3.磺基水楊酸法 實驗九 分光光度法測定阿司匹林藥片的含量 實驗十 分光光度法測定磺基水楊酸合鐵的組成和穩(wěn)定常數(shù) 實驗十一 熒光分析法測定維生素B2的含量 實驗十二 紫外分光光度法對維生素B12的鑒別與含量測定 實驗課題四 化學(xué)原理實驗 實驗十三 稀溶液的依數(shù)性及其應(yīng)用 1.凝固點降低法測定溶質(zhì)的相對分子質(zhì)量 2.利用溶液的滲透濃度測定溶質(zhì)的相對分子質(zhì)量 3.冰點滲透壓計的應(yīng)用 實驗十四 置換法測定鎂的原子量 實驗十五 化學(xué)反應(yīng)速率與活化能的測定 實驗課題五 化合物制備實驗 實驗十六 氯化鈉的精制 實驗十七 硫酸亞鐵銨的制備 實驗課題六 綜合及研究實驗 實驗十八 醋酸解離平衡常數(shù)的測定與市售食醋中HAc含量的測定 實驗十九 茶葉中鈣、鎂和鐵含量的綜合測定 實驗課題七 自行設(shè)計實驗 實驗二十 設(shè)計及研究 Part Ⅰ Experiment Essentials in Basic Chemistry Chapter 1 Laboratory Rules and Safety Information 1. The Purpose of Experiments in Basic Chemistry 2. General Rules in Laboratory 3. Safety Information 4. The Treatment of Accidents in Chemical Experiments 5. Fire Prevention and Extinguishing Knowledge Chapter 2 Ordinary Instruments in Chemical Experiments 1. Ordinary Glassware in Chemical Lab 1.1 Cleaning Glassware 1.2 Drying Glassware 2. Volumetric Glassware 2.1 Burets 2.2 Volumetric Flasks 2.3 Pipets 3. Analytical Instruments 3.1 Analytical Balance 3.2 pH Meter 3.3 721-Speetrophotometer 3.4 FM-9X Osmometer 3.5 Centrifuges Chapter 3 Experiment Results and their Expressions 1. Experimental Error and Significant Figures 1.1 Experimental Error 1.2 Accuracy and Precision 1.3 Significant Figures 2. Treatments of Experimental Data 2.1 Tabling 2.2 Graphing 2.3 Computer treatment 3. Experiment Reports Part Ⅱ Experiments in Basic Chemistry Chapter 1 Basic Practice Experiments of Operation Experiment 1 Operation of Volumetric Analysis Experiment 2 Weighing Practice of Analytical Balance Experiment 3 Preparation and Properties of Buffers and Measure the pH of the Solution Experiment 4 Preparation and Properties of Colloidal Systems Chapter 2 Experiments of Titration Experiment 5 Acid-Base Titration Analysis 1. The Standardization of HC1 Solution Concentration 2. The Standardization of the Concentration of NaOH 3. Determination of Purity of Oxalic Acid 4. Determination of Content of Borax 5. Determination of Aspirin by Back Titration Experiment 6 Oxidation-Reduction Titration 1. Potassium permanganate method 2. Iodimetry Experiment 7 Complexometric Titration 1. Determination of the Hardness of Water 2. Determination Content of KAI(SO4)2·12H20 in Alum 3. Determination of calcium gluconate Chapter 3 Spectrophotometry Experiment 8 Determination of the Content of Fe3 + ( Fe2+) in Water Sample with Spectrophotometry 1. O-phenanthroline Method 2. Sulfocyan (MSCN) Method 3. Sulfosalicylic Acid Method Experiment 9 Determination of the Content of Aspirin in Tablets by Visible Spectrophotometry Experiment 10 Determination of the Formula and the Stability Constant for a sulfosalicylate Iron ( 11I ) Complex by Spectrophotometry Experiment 11 Determination of the Content of Vitamin B2 by Fluorescence Spectrophotometry Experiment 12 Identification and Determination of Vitamin B12 with Ultraviolet Spectrophotometry Chapter 4 Chemical Principle Experiments Experiment 13 Colligative Properties of Dilute Solution and Their Application 1. Determination of Molar Mass of Glucose by Freezing Point Depression 2. Determination of the Molar Mass of Glucose by Determining Osmolarity 3. Application of Freezing Point Osmometer Experiment 14 Determination of the Atomic Mass of Magnesium by Replacement Reaction Experiment 15 Determination of the Rate of Chemical Reaction and Activation Energy Chapter 5 Preparation of Compounds Experiment 16 Refining Sodium Chloride Experiment 17 Preparation of Ammonium Iron (Ⅱ) Sulfate Chapter 6 Comprehensive Experiments Experiment 18 Determination of Dissociation Equilibrium Constant of Acetic Acid and Content of HAc in Commercial Vinegar Experiment 19 Comprehensive Determinations of Content of Ca,Mg and Fe in Tea Chapter 7 Self-Designed Experiment Experiment 20 Design and Research 附錄Ⅰ 國際相對原子量表 附錄Ⅱ 不同溫度下水的飽和蒸汽壓． 附錄Ⅲ 危險藥品的分類、性質(zhì)和管理 一、危險藥品 二、劇毒物品 三、化學(xué)實驗室毒品管理規(guī)定 附錄Ⅳ 標(biāo)準(zhǔn)緩沖溶液 附錄Ⅴ 參考書目